利用传统的水热合成法制备Mo-Ag双金属硫化物：02 g NH4MoS4、013 g AgNO3、80 mL H2O先后加入100 mL聚四氟乙烯内衬的反应釜内胆搅拌30 min内胆放入反应釜加盖拧紧。制备催化剂时在烘箱分别以170 ℃、200 ℃、230 ℃保持12 h自然冷却至室温后将反应釜内胆中的混合溶液离心分离。先后用乙醇胺、蒸馏水洗涤三次最后在真空干燥箱60 ℃真空干燥得到催化剂。翻译成

Synthesis of Mo-Ag bimetallic sulfide using traditional hydrothermal method: 0.2 g NH4MoS4, 0.13 g AgNO3, and 80 mL H2O were sequentially added to the inner liner of a 100 mL reaction vessel lined with polytetrafluoroethylene. The mixture was stirred for 30 min, and then the inner liner was placed into the reaction vessel and tightly sealed. To prepare the catalyst, the reaction vessel was placed in an oven and maintained at 170 ℃, 200 ℃, and 230 ℃ for 12 h each. After cooling to room temperature naturally, the mixed solution in the inner liner of the reaction vessel was separated by centrifugation. The separated material was washed three times with ethanolamine and distilled water, and finally dried in a vacuum drying oven at 60 ℃ to obtain the catalyst