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Thermosetting adhesives are commonly used in various applications. However, their covalent cross-linked network structure makes them difficult to reassemble, requiring higher machining precision. Additionally, the primary raw materials for adhesive preparation are derived from non-renewable petroleum resources, which further limits adhesive development.

In this study, we developed a recyclable adhesive by incorporating dynamic boronic esters into epoxy resin derived from soybean oil (SBO). The successful synthesis of epoxidized soybean oil and boronic esters was confirmed through analysis of 1H NMR spectra and differential scanning calorimetry results. Swelling tests and tensile curves demonstrated the presence of covalent cross-linked networks.

Furthermore, self-healing and reprocessing experiments showed that the cross-linked network topology could be reassembled under mild conditions.

By utilizing dynamic boronic esters and SBO-based epoxy resin, we have created an adhesive that not only possesses recyclability but also exhibits promising mechanical properties